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"/www/wwwroot/web/cache/difa17.com/news.txt" [670]=> string(43) "/www/wwwroot/web/cache/difa17.com/order.txt" [671]=> string(49) "/www/wwwroot/web/cache/difa17.com/products-p2.txt" [672]=> string(49) "/www/wwwroot/web/cache/difa17.com/products-p3.txt" [673]=> string(49) "/www/wwwroot/web/cache/difa17.com/products-p4.txt" [674]=> string(46) "/www/wwwroot/web/cache/difa17.com/products.txt" [675]=> string(42) "/www/wwwroot/web/cache/difa17.com/sale.txt" [676]=> string(43) "/www/wwwroot/web/cache/difa17.com/video.txt" } HAMILTON进样针的使用和维护-上海迪发仪器仪表有限公司
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HAMILTON进样针的使用和维护

更新时间：2011-07-07      点击次数：2088

 

HAMILTON进样针的使用和维护
 
使用注射器进样可以快速选择进样体积并重复的调整（常规±5%的误差，熟练者±1%的误差）当用微升注射器进样时，可遵循如下建议：
1. 运作协调，这样可尽可能快而正准确地注射样品，在压入针杆后注射器在进样口应停留2s。
2. 尽可能靠边缘（表面或无刻度区）握住注射器，这可防止用手指握针筒时的热传递，注射器架可阻止从手指传热，且更容易穿刺隔垫。
3. 用手指接触针杆顶部的纽状物，而不是针杆。这可减小损坏和污染的可能性。
4. 为获得zui大的准确度，进样量要小于注射器的zui大容量，当被注射的样品包含沸点较宽的组分时，可能发生分馏，除非注射器有溶剂塞（用空气泡割开），随样品进入注射口。
5. 在取样入注射器前，通过抽动针杆用样品湿润注射器内表面（针桶或针塞），以确保准确的取样量。
6. 从样品瓶中抽取超过所需进样量的样品，从瓶中抽出注射器，移动针塞至所需刻度线，弃去多余的样品，不可在注射器头附着液滴。
7. 注射前，用无绵纤维檫干净注射针，动作快速，小心不要将注射器中样品吸出，也不要将体热从手指传至针管。
8. 目测检查注射器内气泡或样品中的异物。
9. 当用拆卸针管注射器时，要格外小心，因为针管有死体积，用气密的注射器充满了惰性气体对样品瓶加压，需要时重复此操作，以便在瓶中建立压力。
10.当使用黏性样品时，使用粗孔针头。
11.不要使用钝的或损坏的针头，也5不要将隔垫螺母拧的太紧，否则隔垫寿命将会缩短，由于高温也可以缩短隔垫的寿命，故推荐使用有散热片的螺母来保持低温，所有隔垫zui终会开始泄露，每天换一个隔垫是防止泄露的好措施，分析任务多时要更经常地更换，一些隔垫可以持续150次注射，但在这之前定期更换。
 
上海迪发仪器仪表有限公司为瑞士Hamilton华东区授权代理商，为您提供*的进样针选型指南，更多详情请访问：www.difa17.com，：，技术：，：difabio
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